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@bedseal2
The HPLC apparatus (Infinity 1290 System; Agilent, Mississauga, Ontario, Canada) was outfitted with an Eclipse Plus C18 column (150 mm × 2.1 mm id, 1.8μm; Agilent, Mississauga, Ontario, Canada). The column was eluted with a gradient formed by water and formic acid (0.1%) and acetonitrile . The move fee was zero.35 mL/min, the column t […] View